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University of Oxford
School of Geography and the Environment

 School of Geography and the Environment

Research: Landscape Dynamics: Oxford Rock Breakdown Laboratory

Laboratory and Field Equipment Facilities

Environmental Cabinets

Environmental cabinet Sanyo-FE 300H/MP/R20
Environmental cabinet Sanyo-FE 300H/MP/R20

Description

  • Year: 1975
  • Temperature range of -20 to +100°C
  • Internal dimensions of 675W 630D 650H mm
Environmental cabinet Binder KBF115
Environmental cabinet Binder KBF115

Description:

  • Year: 2005
  • Temperature range of -10 to +100°C
  • Internal dimensions of 600W 400D 480H mm)
  • Electronically controlled APT line™ preheating chamber technology
  • MP controller with 2 programs with 10 sections each, alternatively switchable to 1 program with 20 sections
  • Integrated week program timer with real time function
  • Digital temperature setting with an accuracy of a tenth of a degree
Environmental cabinet Sanyo-MLR-351
Environmental cabinet Sanyo-MLR-351

Description:

  • Year: 2009
  • Temperature range of 0 to 50°C
  • Brightness control range 0 to 20000 Lx with 6 steps changeable
  • Internal dimensions of 520W 490D 1135H mm

Applications:
Used for a broad range of sophisticated applications in laboratories:

  • Arid environmental simulations
  • Rock breakdown and landscape evolution
  • Weathering of historic monuments
  • The effect of bio-soiling on rocks' weathering

Laser Diffraction Particle Sizing

Malvern Master-Sizer 2000
Malvern Master-Sizer 2000

Description:

  • Year: 2008
  • Fully automated
  • Laser diffraction technique and light scattering analyze
  • Measurement of emulsions, suspensions and dry powders
  • Measures materials from 0.02µm to 2000µm
  • Software-driven Standard Operating Procedures (SOPs)

Applications:
Particle and rheological characterization of soil, sediments or powders.

Ion Chromatography System

Dionex IC DX500 Chromatograph
Dionex IC DX500 Chromatograph

Description:

  • Year: 1995, updated
  • GP 40 Gradient Pump
  • CD 20 Conductivity Detector
  • LC20 Chromatogr. Enclosure
  • AS40 Automated Sampler
  • Chromalion Software

Applications:
Determination of inorganic and organic ions in a variety of samples. It is mainly configured for the analysis of the followings anions and cations:
- Chloride, Nitrate, Nitrite, Sulfate, Bromide, Fluoride and Phosphate
- Potassium, Sodium, Calcium, Magnesium.

Non-Destructive Measurement of Elastic Properties of Materials

Grindosonic MK5 'Industrial'
Grindosonic MK5 'Industrial'

Description:

  • Year: 1980
  • Impulse excitation technique
  • Frequency range 20 Hz - 100 KHz
  • Reference accuracy better than 0.005%
  • Piezo-electric vibration detector
  • Acoustic vibration detector
  • Sample size from less than 100 mg to over a ton
  • Modulus values from 0,05 to over 900 GPa
  • E-modulus calculation software

Applications:
Measurement of elastic properties of rocks and others materials.

Non-Destructive Measurement of Rocks with Portable Hardness Testers

Proceq Equotip 3 and Proceq Equotip Piccolo Bambino 2
Proceq Equotip 3 Proceq Equotip piccolo bambino 2

Description:

  • Proceq Equotip 3 - Year: 2008
  • Proceq Equotip Piccolo Bambino 2 - Year: 2011
  • Dynamic Leeb rebour technique
  • Direct conversion to all common hardness scales (HV, HB, HRC, HRB, HRA, HS, Rm)
  • Accuracy ± 4 HL (0.5% at 800 HL) with automatic correction for impact direction
  • Wide measurement range
  • Accurate also on curved test surfaces (R > 10 mm)
  • Down-/upload data from/to PC via USB, Ethernet or RS-232
  • Accurate also on curved test surfaces (R > 10 mm)

Applications:
Measurements of the hardness on a wide selection of materials such as rocks, metals on-site or in lab controlled conditions (humidity, temperature).

Non-Destructive Measurement of Rocks Compressive Strength

Silver Schmidt Hammer
Silver Schmidt Hammer

Description:

  • Range of 10 to 70 MPa (N/mm2) (1'450 to 10'152 psi)
  • Rebound values are read from a scale for subsequent calculation of the mean. Compressive strength values can be read from a conversion diagram

Applications:
Used for the non-destructive measurement of the rocks, concrete/mortar compressive strength characteristics; control of uniform material quality; and the detection of weak spots in the material.

Optical Microscopic System

Meiji ML900 - DeltaPix DP300 Camera and Software
Meiji ML900 - DeltaPix DP300 Camera

Description:

  • Year: 2004-2008
  • Polarizing Microscope
  • Binocular Head with Eyepieces HWF10X and focusing HWF10XF with cross-line reticule
  • 4X, 10X and 40X(S) objectives
  • Deltapix Microscope Camera with 1 to 5000 times magnification, resolves details down to 0.4µm

Applications:
View of rocks and soils in thin sections; and image analysis.

Leica MZ10 F Stereomicroscope
Leica MZ10 F Stereomicroscope

Description:

  • Year: 2011
  • Zoom ratio 10:1
  • Optics carrier magnification 0.8 - 8
  • Design principle Common Main Objective (CMO) optical system
  • Standard magnification 8- 80 (10x eyepieces + 1.0 objective)
  • Standard objective Planapochromatic objective 1.0 (NA = 0.125)
  • Illumination TrippleBeamTM - 3rd (separate) illumination beam path, adapts automatically (via zoom) to Field of View (FOV)
  • Filter changer FLUOIIITM - 4 position, manual
  • Illumination control Manual excitation shutter
  • FOV diameter 131 - 1.31mm (max/min)
  • Resolution (max) 1.33 (750lp/mm)
  • Numerical aperture 0.25 (max)
  • Ratch positions 1 / 1.6 / 2 / 2.5 / 3.2 / 4 / 5 / 6.3

Applications:
Rocks surfaces and inspection for cracks and pores, soft wall capping and plant cells, soil samples, genetics detecting cellular expression. Image analysis.

Leica S8 APO
Leica S8 APO

Description:

  • Year: 2011
  • Apochromatic optics system 8:1
  • Apochromatic objectives
  • Maximum resolution 600 lp/mm
  • 10-80 magnification, working distance 75mm*
  • Video/photo output
  • Adjustable upper and lower zoom magnification stops

Applications:
Rocks surfaces and inspection for cracks and pores, soft wall capping and plant cells, soil samples, genetics detecting cellular expression. Image analysis.

Colour Analysis

Spectrophotometer, CM-700d
Spectrophotometer, CM-700d

Description:

  • Year: 2010
  • Illumination / viewing system - di: 8°, de: 8° (diffused illumination, 8-degree viewing angle), SCI (specular component included)/SCE (specular component excluded), selectable with automatic switching (Conforms to CIE No. 15, ISO 7724/1, DIN5033 Teil7, ASTM E 1164, and JIS Z 8722)
  • Detector - Silicon photodiode array (dual 36-element)
  • Wavelength - range 400 nm to 700 nm
  • Reflectance - range 0 to 175%, Display resolution: 0.01%
  • Repeatability - Spectral reflectance: Standard deviation within 0.1%, Chromaticity value: Standard deviation within ΔE*ab 0.04. When a white calibration plate is measured 30 times at 10-second intervals after white calibration
  • Inter-instrument agreement - Within ΔE*ab 0.2 (MAV/SCI). Based on 12 BCRA Series II color tiles compared to values measured with a master body at 23°C
  • Illuminant - A, C, D50, D65, F2, F6, F7, F8, F10, F11, F12 (Simultaneous evaluation with two light sources possible)
  • Displayed data - Spectral values/graph, colorimetric values, color difference values/graph, PASS/FAIL result, pseudocolor, color
  • Colour spaces - L*a*b*, L*C*h, Hunter Lab, Yxy, XYZ, Munsell, and color difference in these spaces (except for Munsell)
  • Colorimetric data - MI, WI(ASTM E313-73/E313-96), YI(ASTM E313-73/ASTM D1925), ISO Brightness, 8°gloss value
  • Color difference formulas - ΔE*ab (CIE1976), ΔE*94 (CIE1994), ΔE00 (CIE 2000), CMC (l: c)

Atomic Absorption Spectroscopy

Varian SpectrAA 220 FS
Varian SpectrAA 220 FS

Description:

  • Year: 2011
  • Burner- Atomizer : Changeable, laminar, adjustable, optional N2O, premix universal atomizer with fully adjustable nebulizer, fully shielded flame with double-skin chimney
  • Windows-based software; multitasking; multielement; software choice of 11 QC tests or full EPA and userdefinable tests; optional software to assist with compliance with FDA 21 CFR Part 11; range of optional accessories, including saMple introduction pump
  • FORMAT (WAVELENGTH, nm) 1 channel, double beam - for more information please see comments.1 channel, double beam, time-shared, rotating-beam combiner
  • Fast (2 msec) deuterium arc lamp to 2.3 absorbance units, 185-425 nm, electronic beam balance 2
  • Wavelength Range, nm (UV Radiation): 180-900
  • Resolution (nm) : 0.2, 0.5, 1; 0.5 reduced
  • Hammer instantaneous programmable control; interlocks on power, gas, burner present, burner type, flame, spraychamber bung, flame shield, liquid trap; cutoff solenoids external to instrument case With automatic attenuation
  • Detection limits (ppb): Ca (0.4), Cu (0.15), Li (0.9), Mg (0.3), Pb (0.1), Ni (0.38)
  • 4 lamps, automatic select mirror, warm up capability, coded, noncoded; optional UltrAA (boosted) lamp
  • A fully automated double beam system
  • Fast Sequential operation

Applications:
Analytical Technique for determining the concentration of particular metal elements within a sample. It is often used for water, soil, rock samples to determine the alkali, earth-alkali metals as well as heavy metals such as lead, iron and cadmium.

Manual Chop Abrasive Precision Cutter

Delta Buehler
Delta Buehler

Description:

  • Year: 2009
  • Precision cutter
  • Large viewing window and lighted cutting chamber
  • Cutting operation monitored externally
  • Excellent quick and consistent cuts

Applications:
Precision rocks' cutting.

MET Station

(associated with English Heritage projects)

Campbell Scientific Basic Weather Station
Campbell Scientific Basic Weather Station

Description:

  • Year: 2006
  • Weatherproof enclosure mounted on a pole
  • With Datalogger 12V power supply
  • Radiation shield
  • Solar panel
  • Temperature and humidity probe
  • Wind speed and direction sensors
  • Tipping bucket raingauge

Applications:
Climate Changes monitoring.

Electric Resistivity Tomography (ERT)

GeoTom by Geolog2000
GeoTom by Geolog2000

Description:

  • Year: 2007
  • Portable field equipment
  • Can be used on a variety of scales
  • Non-destructive in situ measurements are ideal for historical surfaces
  • Recently added cables include a small scale set transect (5mm)
  • Used in conjunction with RES2DInv and RES3Dinv inversion software

Applications:
Measurement of moisture levels within a solid sample body, such as walls and natural rock outcrops. Used to identify moisture accumulation but also monitor movement over extended periods of time. Individual measurements are compiled in a data set which is then inverted using RES2Dinv or RES3Dinv depending on which application method is required giving the highest probable resistivity distribution.

Other Equipment

  • Dataloggers: Gemini Tiny tag temperature, RH, leaf wetness probes
    • Internal (material) or External (ambient)
    • Log temperature and humidity
    • 32,000 readings capacity
    • USB or serial download cables
  • Dataloggers: ibutton temperature, RH
    • Extremely small and rugged
    • External (ambient) recording
    • Log temperature and humidity
    • 8,000 readings capacity
    • PC Programmable
  • Data loggers-based telemetric logging system for soil moisture and temperature, Eltek Squirrel
  • Water permeability testing: Proceq Karsten tubes
  • Conductivity meter
  • pH meter
  • InfraRed 2D Thermometer Tech-Jam TJ-200
  • Scanning Electron Microscope Cambrigde Stereoscan 90 (Arrange use with Dr Peter Bull)
  • Camera system: EOS 1000D equipped with macro lenses
  • Rock saw Diamant-Boart TS500M M157/1
  • Original Schmidt Hammer Type N